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Synthesis of p-Xylenechloride from Toluene by Chloromethylation

Memoirs of the Faculty of Engineering, Yamaguchi University Volume 15 Issue 1 Page 67-69
published_at 1965
KJ00000155526.pdf
[fulltext] 137 KB
Title
トルエンのクロルメチル化反応によるパラキシレンクロリドの合成
Synthesis of p-Xylenechloride from Toluene by Chloromethylation
Creators Murata Sunao
Creators Fuzisaki Shizuo
Creators Mako Isao
Source Identifiers
p-Xylenechloride which can be converted to terephthalic acid for polyester use by oxidation was prepared from toluene by chloromethylation (by treatment with formalin, HCI, & ZnCI_2). The best results were followed : Toluene 2.2 mol, Formalin 1.2 mol, HCI speed passed 440ml/min, Time 2 hrs, Temp. 70°±2°C, Yield 68.5%.
Subjects
化学工学 ( Other)
Languages jpn
Resource Type departmental bulletin paper
Publishers 山口大学工学部
Date Issued 1965
File Version Version of Record
Access Rights open access
Relations
[ISSN]0372-7661
[NCID]AN00244228
Schools 工学部